Hexobarbital (Pharmaceuticals)
Chiral separation on MEGA-DEX columns
Column: MEGA-DEX DMP Beta – 0.25mm, 0.25μm, 25m
Catalog Code: DEX-DMP-B-025-025-25
Conditions:
Injection: Split 250°C, 0.5 μL, 1:50 Split Ratio.
Sample dilution: 1 mg/mL in n-Hexane.
Detector: FID, 250°C.
Oven Temp.: 100°C, 2.5°C/min, 170°C.
Carrier Gas: Hydrogen, 70 kPa
Peaks:
1.. (+) Hexobarbital
2. (-) Hexobarbital
